A Convenient and Practical Method for the Synthesis of Aromatic Nthiophosphoryl Imines

Xinyuan      Xu; Chungui      Wang; Zhenghong      Zhou; Zebing      Zeng; Xinpeng      Ma; Guofeng      Zhao; Chuchi      Tang

doi:10.2174/157017806778559446

Abstract

Thermal condensation of acetals with different thiophosphoramides at 120-160 °C resulted in the formation of the corresponding N-thiophosphoryl imines in good to excellent yield (80-98%) with high purity ( > 95%, determined by 1H NMR and elemental analyses).

Keywords: N-Thiophosphoryl imine, thermal condensation, thiophosphoramide, acetal

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Letters in Organic Chemistry

Title: A Convenient and Practical Method for the Synthesis of Aromatic Nthiophosphoryl Imines

Volume: 3 Issue: 8

Author(s): Xinyuan Xu, Chungui Wang, Zhenghong Zhou, Zebing Zeng, Xinpeng Ma, Guofeng Zhao and Chuchi Tang

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Keywords: N-Thiophosphoryl imine, thermal condensation, thiophosphoramide, acetal

Abstract: Thermal condensation of acetals with different thiophosphoramides at 120-160 °C resulted in the formation of the corresponding N-thiophosphoryl imines in good to excellent yield (80-98%) with high purity ( > 95%, determined by 1H NMR and elemental analyses).

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Xu Xinyuan, Wang Chungui, Zhou Zhenghong, Zeng Zebing, Ma Xinpeng, Zhao Guofeng and Tang Chuchi, A Convenient and Practical Method for the Synthesis of Aromatic Nthiophosphoryl Imines, Letters in Organic Chemistry 2006; 3 (8) . https://dx.doi.org/10.2174/157017806778559446