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Current Nanomaterials

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ISSN (Print): 2405-4615
ISSN (Online): 2405-4623

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Research Article

Surface Characterization of Zinc Oxide Nanoparticles Synthesized via Chemical Route

Author(s): Soamyaa Srivastava* and Jayanand Manjhi

Volume 8, Issue 2, 2023

Published on: 01 August, 2022

Page: [175 - 181] Pages: 7

DOI: 10.2174/2405461507666220603115619

Price: $65

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Abstract

Introduction: Zinc oxide nanoparticles belong to the new age of nanomaterials; they are being used tremendously for the advancements of biomedicine and modern therapeutic interventions.

Purpose: The current antimicrobial treatment methods fail on various levels. Thus, the recent study is dedicated to synthesizing stable zinc oxide nanoparticles. Therefore, the application of zinc oxide nanoparticles as an alternative treatment option is explored.

Methods: In the current research, fabrication of zinc oxide nanoparticles is carried out via the wet chemical method. To further confirm the purity and stability of the synthesized material, characterization was performed via zeta potential analysis, thermogravimetric analysis, differential scanning calorimetry, transmission electron microscopy and scanning electron microscopy.

Results: SEM and TEM revealed the spherical structure of zinc oxide nanoparticles, also having slight agglomeration at a few points. The thermal stability was tested via thermogravimetric analysis and differential Scanning Calorimetry depicting the strength of the nanomaterial at a very high temperature. Elemental composition was evaluated using Energy Dispersive X-ray Spectroscopy showing 96.01% zinc and 3.99% oxygen, demonstrating the purity of the synthesized zinc oxide nanoparticles. It confirms that no other elements are present apart from zinc and oxygen.

Conclusion: Zinc oxide nanoparticles were synthesized via a wet chemical method using zinc nitrate and sodium hydroxide. This fabrication procedure is reliable, cheap, and yields the most stable byproducts. Characterization was carried out via several analytical techniques to check the authenticity of the synthesized nanomaterial, thus revealing that the obtained ZnO nanoparticles could be used in medical interventions as a safe option.

Keywords: ZnO nanoparticles, wet chemical method, differential scanning calorimetry, energy dispersive X-ray spectroscopy, transmission electron microscopy.

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[1]
Tiller JC, Liao CJ, Lewis K, Klibanov AM. Designing surfaces that kill bacteria on contact. Proc Natl Acad Sci 2001; 98(11): 5981-5.
[http://dx.doi.org/10.1073/pnas.111143098] [PMID: 11353851]
[2]
Thill A, Zeyons O, Spalla O, et al. Cytotoxicity of CeO2 nanoparticles on Escherichia Coli: Physiochemical insight of cytotoxicity mechanism. Environ Sci Technol 2006; 40: 6151.
[http://dx.doi.org/10.1021/es060999b] [PMID: 17051814]
[3]
Jones N, Ray B, Ranjit KT, Manna AC. Antibacterial activity of ZnO nanoparticle suspensions on a broad spectrum of microorganisms. FEMS Microbiol Lett 2008; 279(1): 71-6.
[http://dx.doi.org/10.1111/j.1574-6968.2007.01012.x] [PMID: 18081843]
[4]
Brayner R, Ferrari-Iliou R, Brivois N, Djediat S, Benedetti MF, Fiévet F. Toxicological impact studies based on Escherichia coli bacteria in ultrafine ZnO nanoparticles colloidal medium. Nano Lett 2006; 6(4): 866-70.
[http://dx.doi.org/10.1021/nl052326h] [PMID: 16608300]
[5]
Desselberger U. Emerging and re-emerging infectious diseases. J Infect 2000; 40(1): 3-15.
[http://dx.doi.org/10.1053/jinf.1999.0624] [PMID: 10762105]
[6]
Morones JR, Elechiguerra JL, Camacho A, et al. The bactericidal effect of silver nanoparticles. Nanotechnology 2005; 16(10): 2346-53.
[http://dx.doi.org/10.1088/0957-4484/16/10/059] [PMID: 20818017]
[7]
Sawai J. Quantitative evaluation of antibacterial activities of metallic oxide powders (ZnO, MgO and CaO) by conductimetric assay. J Microbiol Methods 2003; 54(2): 177-82.
[http://dx.doi.org/10.1016/S0167-7012(03)00037-X] [PMID: 12782373]
[8]
Seil JT, Webster TJ. Antimicrobial applications of nanotechnology: Methods and literature. Int J Nanomed 2012; 7: 2767-81.
[PMID: 22745541]
[9]
Ramani M, Ponnusamy S, Muthamizhchelvan C. From zinc oxide to micro flowers: A study of Growth kinetics and biocidal activity. Mater Sci Eng C 2012; 32(8): 2381-9.
[http://dx.doi.org/10.1016/j.msec.2012.07.011]
[10]
Kim KM, Kim TH, Kim HM, et al. Colloidal behaviors of ZnO nanoparticles in various aqueous media. Toxicol Environ Health Sci 2012; 4(2): 121-31.
[http://dx.doi.org/10.1007/s13530-012-0126-5]
[11]
Kim KM, Choi MH, Lee JK, et al. Physicochemical properties of surface charge-modified ZnO nanoparticles with different particle sizes. Int J Nanomed 2014; 9(2) (Suppl. 2): 41-56.
[PMID: 25565825]
[12]
Kumar H, Rani R. Structural and optical characterization of ZnO nanoparticles synthesized by microemulsion route. Int Lett Chem Phys Astron 2013; 14: 26-36.

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