Abstract
Chemspeed’s AUTOPLANT ZEO Robotic Platform together with the Workflow Management Software provides faster and better zeolite synthesis. Reproducibilities over 20 fully automated 100mL reactors per run are within ±5%. The physico-chemical properties of zeolites produced proved to be scalable to 2-Liter stainless-steel autoclave. Varying a suite of raw materials with different physicochemical properties, the ratios of n(SDA)/n(SiO2) and the ratios of n(H2O)/n(SiO2), the productivity could be increased by a factor of 10. Zeolites were reproducibly synthesized in high solid-content (viscous) regimes.
Keywords: Zeolites, synthesis, reproducibility, scalability, downscaling, upscaling, high output, automated.
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