Silica Sulfuric Acid-Catalyzed Syntheses of Calix[4] Resorcinarenes

Ling-ling      Zhaoa; Yu      Wan; Shu-ying      Huang; Gui-xiang      Liu; Liang-feng      Chen; Shu-ning      Yue; Wen-li      Zhang; Hui      Wu

doi:10.2174/1570178611310040012

Abstract

Silica sulfuric acid (SSA) was firstly used as an efficient catalyst to promote the synthesis of rctt configurational calix[4]resorcinarenes via one-pot condensation between resorcinol and aromatic aldehydes. The structure of 4- cyanophenyl-calix[4]resorcinarene (3b) has been determined by single crystal X-ray diffraction.

Keywords: Silica sulfuric acid, Calix[4]resorcinarenes.

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Letters in Organic Chemistry

Title:Silica Sulfuric Acid-Catalyzed Syntheses of Calix[4] Resorcinarenes

Volume: 10 Issue: 4

Author(s): Ling-ling Zhaoa, Yu Wan, Shu-ying Huang, Gui-xiang Liu, Liang-feng Chen, Shu-ning Yue, Wen-li Zhang and Hui Wu

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Keywords: Silica sulfuric acid, Calix[4]resorcinarenes.

Abstract: Silica sulfuric acid (SSA) was firstly used as an efficient catalyst to promote the synthesis of rctt configurational calix[4]resorcinarenes via one-pot condensation between resorcinol and aromatic aldehydes. The structure of 4- cyanophenyl-calix[4]resorcinarene (3b) has been determined by single crystal X-ray diffraction.

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Zhaoa Ling-ling, Wan Yu, Huang Shu-ying, Liu Gui-xiang, Chen Liang-feng, Yue Shu-ning, Zhang Wen-li and Wu Hui, Silica Sulfuric Acid-Catalyzed Syntheses of Calix[4] Resorcinarenes, Letters in Organic Chemistry 2013; 10 (4) . https://dx.doi.org/10.2174/1570178611310040012