Highly Efficient Kinetic Resolution of Allylic Alcohols with Terminal Double Bond

Francisco      A. Marques; Marcos      A. Oliveira; Gustavo      Frensch; Beatriz      Helena L. N. Sales Maia; Andersson      Barison; Cesar      A. Lenz; Palimecio      G. Guerrero

doi:10.2174/157017811799304151

Abstract

In this study, the lipase-catalyzed kinetic resolution (Novozyme 435) was employed to prepare chiral allylic alcohols and acetates with terminal double bonds in enantiomeric excesses ranging from 94 to > 99 %.

Keywords: Allylic alcohols and acetates, fragrances, pheromones, agrochemicals, high enantiomeric exces, kinetic resolution, Novozyme 435, alcohols, allenols

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Letters in Organic Chemistry

Title: Highly Efficient Kinetic Resolution of Allylic Alcohols with Terminal Double Bond

Volume: 8 Issue: 10

Author(s): Francisco A. Marques, Marcos A. Oliveira, Gustavo Frensch, Beatriz Helena L. N. Sales Maia, Andersson Barison, Cesar A. Lenz and Palimecio G. Guerrero

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Keywords: Allylic alcohols and acetates, fragrances, pheromones, agrochemicals, high enantiomeric exces, kinetic resolution, Novozyme 435, alcohols, allenols

Abstract: In this study, the lipase-catalyzed kinetic resolution (Novozyme 435) was employed to prepare chiral allylic alcohols and acetates with terminal double bonds in enantiomeric excesses ranging from 94 to > 99 %.

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A. Marques Francisco, A. Oliveira Marcos, Frensch Gustavo, Helena L. N. Sales Maia Beatriz, Barison Andersson, A. Lenz Cesar and G. Guerrero Palimecio, Highly Efficient Kinetic Resolution of Allylic Alcohols with Terminal Double Bond, Letters in Organic Chemistry 2011; 8 (10) . https://dx.doi.org/10.2174/157017811799304151