Synthesis of 1,3-Dithiole-2-thione-4,5-dithiolate-Carbohydrate Conjugate

Angelica   M.   Heinrich; Shahnaz      Perveen; Khalid   M.   Khan; Gerardo   C.   Janairo; Gernot      Bruchelt; Syed   Tasadaque Ali   Shah; Wolfgang      Voelter

doi:10.2174/157017809788489873

Abstract

Bis(tetraethylammonium)bis(1,3-dithiole-2-thione-4,5-dithiolato) zincate (5), and 4,5-bis(cyanoethylthio)-1,3- dithiole-2-thione (6) were reacted with 6-deoxy-6-iodo-glucopyranose (2) and glucopyranosyl bromide (3) to synthesize DMIT-carbohydrate conjugates.

Keywords: Bis(tetraethylammonium)bis(1,3-dithiole-2-thione-4,5-dithiolato) zincate, 4,5-Bis(cyanoethylthio)-1, 3-dithiole-2-thione, 1,3-Dithiole-2-thione-4, 5-dithiolate-carbohydrate conjugates

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Letters in Organic Chemistry

Title: Synthesis of 1,3-Dithiole-2-thione-4,5-dithiolate-Carbohydrate Conjugate

Volume: 6 Issue: 4

Author(s): Angelica M. Heinrich, Shahnaz Perveen, Khalid M. Khan, Gerardo C. Janairo, Gernot Bruchelt, Syed Tasadaque Ali Shah and Wolfgang Voelter

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Keywords: Bis(tetraethylammonium)bis(1,3-dithiole-2-thione-4,5-dithiolato) zincate, 4,5-Bis(cyanoethylthio)-1, 3-dithiole-2-thione, 1,3-Dithiole-2-thione-4, 5-dithiolate-carbohydrate conjugates

Abstract: Bis(tetraethylammonium)bis(1,3-dithiole-2-thione-4,5-dithiolato) zincate (5), and 4,5-bis(cyanoethylthio)-1,3- dithiole-2-thione (6) were reacted with 6-deoxy-6-iodo-glucopyranose (2) and glucopyranosyl bromide (3) to synthesize DMIT-carbohydrate conjugates.

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Heinrich M. Angelica, Perveen Shahnaz, Khan M. Khalid, Janairo C. Gerardo, Bruchelt Gernot, Shah Tasadaque Ali Syed and Voelter Wolfgang, Synthesis of 1,3-Dithiole-2-thione-4,5-dithiolate-Carbohydrate Conjugate, Letters in Organic Chemistry 2009; 6 (4) . https://dx.doi.org/10.2174/157017809788489873