Synthesis of 14-Membered Ring Jaspamide Derivatives

S.      Celanire; C.      Descamps-Francois; B.      Lesur; G.      Guillaumet; B.      Joseph

doi:10.2174/1570178054640697

Abstract

Two synthetic approaches of simpler jaspamide derivatives were investigated. The ring closure step was attempted either by RCM or by macrolactonisation. 14-Membered ring derivatives 15-16 were prepared by final macrolactonisation using Yamaguchi reagent.

Keywords: alkaloid, macrocycle, olefin metathesis, macrolactonisation

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Letters in Organic Chemistry

Title: Synthesis of 14-Membered Ring Jaspamide Derivatives

Volume: 2 Issue: 6

Author(s): S. Celanire, C. Descamps-Francois, B. Lesur, G. Guillaumet and B. Joseph

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Keywords: alkaloid, macrocycle, olefin metathesis, macrolactonisation

Abstract: Two synthetic approaches of simpler jaspamide derivatives were investigated. The ring closure step was attempted either by RCM or by macrolactonisation. 14-Membered ring derivatives 15-16 were prepared by final macrolactonisation using Yamaguchi reagent.

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Celanire S., Descamps-Francois C., Lesur B., Guillaumet G. and Joseph B., Synthesis of 14-Membered Ring Jaspamide Derivatives, Letters in Organic Chemistry 2005; 2 (6) . https://dx.doi.org/10.2174/1570178054640697