Studies on Crystal Engineering Networks of Amidopyridine N-oxides in Solid State by NMR, Mass and X-ray Techniques

Title:Studies on Crystal Engineering Networks of Amidopyridine N-oxides in Solid State by NMR, Mass and X-ray Techniques

Volume: 12 Issue: 8

Author(s): Swapan Dey, Ashish Kumar, Dibyendu Sain, Hari Pada Nayek, Anita Hazra, Shyamaprosad Goswami, Subrata Jana, Hoong-Kun Fun and Samil Isik

Affiliation:

Keywords: Crystal engineering networks, amidopyridine-N-oxide.

Abstract: Four organic compounds, N¹,N⁴-bis(6-methylpyridin-2-yl)terephthalamide (1), its di-Noxide (3), mono-N-oxide with water (5w) and di-N-oxide (6) of N¹,N³-bis(6-methylpyridin-2-yl) (4) have been synthesized and their solid state structures have also been determined using FTIR, NMR, Mass and single crystal X-ray analysis. Three dimensional propagations, conventional and nonconventional hydrogen bonding with their point of interactions, molecular modeling and Hirshfeld surface analysis are discussed in this context.

Cite this article as:

Dey Swapan, Kumar Ashish, Sain Dibyendu, Nayek Pada Hari, Hazra Anita, Goswami Shyamaprosad, Jana Subrata, Fun Hoong-Kun and Isik Samil, Studies on Crystal Engineering Networks of Amidopyridine N-oxides in Solid State by NMR, Mass and X-ray Techniques, Letters in Organic Chemistry 2015; 12 (8) . https://dx.doi.org/10.2174/1570178612666150507222116