Rapid and Efficient Synthesis of N-alkylbenzamides Under Microwave Irradiation

Jan      K. Cermak; Karel      Kolar; Vladimir      Cirkva

doi:10.2174/1570178611310020011

Abstract

The microwave-assisted synthesis of N-alkylbenzamides from benzoic acid and primary aliphatic amines has been developed under solvent-free conditions. The different solid catalysts have been investigated. The suggested synthesis is environmentally friendly and excellent yields (97 - 99 %) have been reached.

Keywords: Amino-de-hydroxylation, heterogenous catalyst, microporous materials, microwave assisted synthesis, Nalkylbenzamides, solvent-free reaction

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Letters in Organic Chemistry

Title:Rapid and Efficient Synthesis of N-alkylbenzamides Under Microwave Irradiation

Volume: 10 Issue: 2

Author(s): Jan K. Cermak, Karel Kolar and Vladimir Cirkva

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Keywords: Amino-de-hydroxylation, heterogenous catalyst, microporous materials, microwave assisted synthesis, Nalkylbenzamides, solvent-free reaction

Abstract: The microwave-assisted synthesis of N-alkylbenzamides from benzoic acid and primary aliphatic amines has been developed under solvent-free conditions. The different solid catalysts have been investigated. The suggested synthesis is environmentally friendly and excellent yields (97 - 99 %) have been reached.

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K. Cermak Jan, Kolar Karel and Cirkva Vladimir, Rapid and Efficient Synthesis of N-alkylbenzamides Under Microwave Irradiation, Letters in Organic Chemistry 2013; 10 (2) . https://dx.doi.org/10.2174/1570178611310020011