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Micro and Nanosystems

Editor-in-Chief

ISSN (Print): 1876-4029
ISSN (Online): 1876-4037

A Review of Recent In Situ Deformation Studies Using Synchrotron X-Ray (Micro) Beams

Author(s): Alexander M. Korsunsky, Felix Hofmann, Xu Song, Brian Abbey and Nikolaos Baimpas

Volume 4, Issue 2, 2012

Page: [97 - 105] Pages: 9

DOI: 10.2174/1876402911204020097

Price: $65

Abstract

The advent of (sub)microscopic focused X-ray beams at third generation synchrotron sources has opened up possibilities for the characterisation of material structure and mechanical behaviour with unprecedented spatial resolution. Crucially, the non-destructive nature and fast rate of X-ray data collection allow in situ deformation to be studied. In this review, we concentrate on the inelastic deformation response of ductile metallic (poly)crystals. We describe a range of diffraction-based techniques we have developed including monochromatic beam reciprocal space mapping, scanning “pink” beam micro-diffraction compound topography, and white beam Laue micro-diffraction. We compare the results obtained using each of the above techniques, and assess and review the insights that they afford into micro-scale material deformation.

Keywords: Synchrotron, X-ray diffraction, micro-beam, dislocation


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