Efficient Synthesis of Wang Resin-Supported 6-O-Benzylallosamizoline

Gangliang      Huang; Qin      Yang

doi:10.2174/157017810791514698

Abstract

An efficient procedure of flash heating by microwave irradiation was described for the attachment of 6-O-benzylallosamizoline 8 to chloromethylated Wang resin 7 via its corresponding stannylene intermediate. The reaction rate and loading for compound 8 were significantly enhanced when the microwave irradiation protocol was compared with the conventional heating method.

Keywords: Wang resin-supported 6-O-benzylallosamizoline, synthesis, stannylene method, microwave irradiation, conventional heating method

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Letters in Organic Chemistry

Title: Efficient Synthesis of Wang Resin-Supported 6-O-Benzylallosamizoline

Volume: 7 Issue: 5

Author(s): Gangliang Huang and Qin Yang

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Keywords: Wang resin-supported 6-O-benzylallosamizoline, synthesis, stannylene method, microwave irradiation, conventional heating method

Abstract: An efficient procedure of flash heating by microwave irradiation was described for the attachment of 6-O-benzylallosamizoline 8 to chloromethylated Wang resin 7 via its corresponding stannylene intermediate. The reaction rate and loading for compound 8 were significantly enhanced when the microwave irradiation protocol was compared with the conventional heating method.

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Huang Gangliang and Yang Qin, Efficient Synthesis of Wang Resin-Supported 6-O-Benzylallosamizoline, Letters in Organic Chemistry 2010; 7 (5) . https://dx.doi.org/10.2174/157017810791514698