Efficient Microwave and Phosphane-Free Synthesis of Trisubstituted Olefins via Heck Coupling

Guya      Loddo; Ornella      Azzolina; Andrea      Magnani; Mariangela      Urbano; Simona      Collina

doi:10.2174/157017806774964549

Abstract

We describe an easy and convenient procedure for palladium-catalyzed Heck arylation of disubstituted olefins via microwave irradiation. This method of synthesis produces trisubstituted olefins under phosphane-free conditions and in very short times.

Keywords: microwave irradiation, chemical library, phosphane-free procedure, trisubstituted olefins, Heck reaction

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Letters in Organic Chemistry

Title: Efficient Microwave and Phosphane-Free Synthesis of Trisubstituted Olefins via Heck Coupling

Volume: 3 Issue: 1

Author(s): Guya Loddo, Ornella Azzolina, Andrea Magnani, Mariangela Urbano and Simona Collina

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Keywords: microwave irradiation, chemical library, phosphane-free procedure, trisubstituted olefins, Heck reaction

Abstract: We describe an easy and convenient procedure for palladium-catalyzed Heck arylation of disubstituted olefins via microwave irradiation. This method of synthesis produces trisubstituted olefins under phosphane-free conditions and in very short times.

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Loddo Guya, Azzolina Ornella, Magnani Andrea, Urbano Mariangela and Collina Simona, Efficient Microwave and Phosphane-Free Synthesis of Trisubstituted Olefins via Heck Coupling, Letters in Organic Chemistry 2006; 3 (1) . https://dx.doi.org/10.2174/157017806774964549