Abstract
A facile microwave heating method was applied to the preparation of nickel-dimethylglyoxime microtubes in half an hour, using nickel nitrate and diacetyldioxime as starting reagents, in the absence of template or surfactant. The products were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM) and infrared spectroscopy (IR). Results show that those microtubes with lengths of 100-500 µm and diameters of 10-15 µm are hollowed. Furthermore, these microtube are hollowed via an inside to outside process under microwave irradiation. For comparison, experiments were carried out under refluxing conditions.
Keywords: Coordination polymers, drug delivery, microstructure, microtubes, microwave, MOFs, nickel, nanoscale, ultralong, soft materials.
Graphical Abstract
Current Microwave Chemistry
Title:Ultralong Coordination Polymers Microtubes: Facile Microwave Preparation and Characterization
Volume: 1 Issue: 1
Author(s): Yanhua Ji, Haiming Yan, Lei Wang, Yuwen Luo, Dongdong Guo, Linjie Bai and Shengliang Zhong
Affiliation:
Keywords: Coordination polymers, drug delivery, microstructure, microtubes, microwave, MOFs, nickel, nanoscale, ultralong, soft materials.
Abstract: A facile microwave heating method was applied to the preparation of nickel-dimethylglyoxime microtubes in half an hour, using nickel nitrate and diacetyldioxime as starting reagents, in the absence of template or surfactant. The products were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM) and infrared spectroscopy (IR). Results show that those microtubes with lengths of 100-500 µm and diameters of 10-15 µm are hollowed. Furthermore, these microtube are hollowed via an inside to outside process under microwave irradiation. For comparison, experiments were carried out under refluxing conditions.
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Cite this article as:
Ji Yanhua, Yan Haiming, Wang Lei, Luo Yuwen, Guo Dongdong, Bai Linjie and Zhong Shengliang, Ultralong Coordination Polymers Microtubes: Facile Microwave Preparation and Characterization, Current Microwave Chemistry 2014; 1 (1) . https://dx.doi.org/10.2174/2213335601666131223234744
DOI https://dx.doi.org/10.2174/2213335601666131223234744 |
Print ISSN 2213-3356 |
Publisher Name Bentham Science Publisher |
Online ISSN 2213-3364 |
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