Ritter Reaction in Subcritical Water: An Efficient and Green Method for Amides Synthesis

Shengqian      Jiang; Zhouyu      Wang; Zhenju      Jiang; Jianhui      Li; Shulin      Zhou; Long      Pu

doi:10.2174/157017812799304006

Abstract

Ritter reaction was carried out efficiently in subcritical water with catalytic amount of trifluoromethanesulfonic acid. The amides were formed in good to excellent yields from secondary alcohols and tert-butanol with various nitriles.

Keywords: Alcohol, amide, nitrile, ritter reaction, subcritical water, trifluoromethanesulfonic acid, chloride, boron trifluoride, sulfuric acid, silica sulfuric acid

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Letters in Organic Chemistry

Title: Ritter Reaction in Subcritical Water: An Efficient and Green Method for Amides Synthesis

Volume: 9 Issue: 1

Author(s): Shengqian Jiang, Zhouyu Wang, Zhenju Jiang, Jianhui Li, Shulin Zhou and Long Pu

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Keywords: Alcohol, amide, nitrile, ritter reaction, subcritical water, trifluoromethanesulfonic acid, chloride, boron trifluoride, sulfuric acid, silica sulfuric acid

Abstract: Ritter reaction was carried out efficiently in subcritical water with catalytic amount of trifluoromethanesulfonic acid. The amides were formed in good to excellent yields from secondary alcohols and tert-butanol with various nitriles.

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Jiang Shengqian, Wang Zhouyu, Jiang Zhenju, Li Jianhui, Zhou Shulin and Pu Long, Ritter Reaction in Subcritical Water: An Efficient and Green Method for Amides Synthesis, Letters in Organic Chemistry 2012; 9 (1) . https://dx.doi.org/10.2174/157017812799304006