Efficient Acetylation and Boc Protection of Carbohydrates, Phenols and Amines

Pintu   Kumar   Mandal; Anup   Kumar   Misra

doi:10.2174/157017808783955880

Abstract

An efficient acetylation and tert-butoxycarbonylation (Boc) of carbohydrate derivatives, phenols and amines catalyzed by tetrabutylammonium bromide is reported. The reaction condition is applicable to substrates containing acid and base labile functional groups. In most of the cases yields obtained were excellent.

Keywords: Carbohydrates, acetylation, tert-butoxycarbonyl, protecting groups, amines, phenols

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Letters in Organic Chemistry

Title: Efficient Acetylation and Boc Protection of Carbohydrates, Phenols and Amines

Volume: 5 Issue: 3

Author(s): Pintu Kumar Mandal and Anup Kumar Misra

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Keywords: Carbohydrates, acetylation, tert-butoxycarbonyl, protecting groups, amines, phenols

Abstract: An efficient acetylation and tert-butoxycarbonylation (Boc) of carbohydrate derivatives, phenols and amines catalyzed by tetrabutylammonium bromide is reported. The reaction condition is applicable to substrates containing acid and base labile functional groups. In most of the cases yields obtained were excellent.

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Mandal Kumar Pintu and Misra Kumar Anup, Efficient Acetylation and Boc Protection of Carbohydrates, Phenols and Amines, Letters in Organic Chemistry 2008; 5 (3) . https://dx.doi.org/10.2174/157017808783955880