Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O

Chun-juan      Shi; Jianbo      Zhang; Jie      Fu; Jie      Tang

doi:10.2174/157017806779468013

Abstract

Several monosaccharides were peracetylated in excellent isolated yields (89-100%) with vinyl acetate in aqueous Na3PO4. The per-O-acetylation reaction is fast and mild, as well as insensitive to water. Meanwhile, the workup is convenient and the catalyst can be recycled easily.

Keywords: Acetylation, monosaccharide, vinyl acetate, catalyst, sodium phosphate

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Letters in Organic Chemistry

Title: Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O

Volume: 3 Issue: 12

Author(s): Chun-juan Shi, Jianbo Zhang, Jie Fu and Jie Tang

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Keywords: Acetylation, monosaccharide, vinyl acetate, catalyst, sodium phosphate

Abstract: Several monosaccharides were peracetylated in excellent isolated yields (89-100%) with vinyl acetate in aqueous Na3PO4. The per-O-acetylation reaction is fast and mild, as well as insensitive to water. Meanwhile, the workup is convenient and the catalyst can be recycled easily.

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Shi Chun-juan, Zhang Jianbo, Fu Jie and Tang Jie, Convenient Per-O-Acetylation of Monosaccharides with Vinyl Acetate/ Na3PO4-H2O, Letters in Organic Chemistry 2006; 3 (12) . https://dx.doi.org/10.2174/157017806779468013