Synthesis of N-Chlorodiazinones Using Sodium Hypochlorite Solution

Osamu      Sugimoto; Satomi      Uchitani; Mizuki      Endo; Ken-ichi      Tanji

doi:10.2174/157017806778559455

Abstract

N-Chlorodiazinones were newly synthesized by reaction of diazinones with sodium hypochlorite in aqueous media in excellent to good yields. Yields of the products varied depending upon the pH value of the solution: in many cases the N-chlorination proceeded more smoothly at pH7 than at pH12.

Keywords: N-chlorination, pyrimidinone, sodium hypochlorite

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Letters in Organic Chemistry

Title: Synthesis of N-Chlorodiazinones Using Sodium Hypochlorite Solution

Volume: 3 Issue: 8

Author(s): Osamu Sugimoto, Satomi Uchitani, Mizuki Endo and Ken-ichi Tanji

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Keywords: N-chlorination, pyrimidinone, sodium hypochlorite

Abstract: N-Chlorodiazinones were newly synthesized by reaction of diazinones with sodium hypochlorite in aqueous media in excellent to good yields. Yields of the products varied depending upon the pH value of the solution: in many cases the N-chlorination proceeded more smoothly at pH7 than at pH12.

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Sugimoto Osamu, Uchitani Satomi, Endo Mizuki and Tanji Ken-ichi, Synthesis of N-Chlorodiazinones Using Sodium Hypochlorite Solution, Letters in Organic Chemistry 2006; 3 (8) . https://dx.doi.org/10.2174/157017806778559455